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Ultrasonic texture characterization of aluminum, zirconium and titanium alloys

机译:铝,锆和钛合金的超声波织构表征

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摘要

This work attempts to show the feasibility of nondestructive characterization of non-ferrous alloys, specifically aluminum, zirconium, and titanium. Aluminum alloys have a small single crystal anisotropy which requires very precise ultrasonic velocity measurements for derivation of orientation distribution coefficients (ODCs); the precision in the ultrasonic velocity measurement required for aluminum alloys is much greater than is necessary for iron alloys or other alloys with a large single crystal anisotropy. To provide greater precision, some signal processing corrections need to be applied to account for the inherent, half-bandwidth offset in triggered pulses when using a zero-crossing technique for determining ultrasonic velocity. In addition, alloys with small single crystal anisotropy show a larger dependence on the single crystal elastic constants (SCECs) when predicting ODCs which require absolute velocity measurements. Attempts were made to independently determine these elastics constants in an effort to improve correlation between ultrasonically derived ODCs and diffraction derived ODCs;The greater precision required to accurately derive ODCs in aluminum alloys using ultrasonic nondestructive techniques is easily attainable. Ultrasonically derived ODCs show good correlation with derivations made by Bragg diffraction techniques, both neutron and X-ray. The best correlations were shown when relative velocity measurements could be used in the derivations of the ODCs. Derivations of W400, which require absolute velocity measurements, were not terribly good, but this is because the SCECs strongly influence these derivations. Once the SCECs were independently determined for the particular alloy studied, the computations of W400 improved;Calculation of ODCs in materials with hexagonal crystallites can also be done. Because of the crystallite symmetries, more information can be extracted using ultrasonic techniques, but at a cost of requiring more physical measurements. Some industries which use materials with hexagonal crystallites, e.g. zirconium alloys and titanium, have traditionally used texture parameters which provide some specialized measure of the texture. These texture parameters, called Kearns factors, can be directly related to ODCs. Again, good correlations between ultrasonically determined ODCs and diffraction determined ODCs were found. In addition, Kearns parameters derived using ultrasonic techniques correlated well with Kearns parameters derived using neutron and X-ray diffraction.
机译:这项工作试图证明非铁合金,特别是铝,锆和钛的非破坏性表征的可行性。铝合金具有较小的单晶各向异性,因此需要非常精确的超声速度测量才能得出取向分布系数(ODC)。铝合金所需的超声速度测量精度远高于铁合金或其他具有大单晶各向异性的合金。为了提供更高的精度,当使用零交叉技术确定超声速度时,需要应用一些信号处理校正来解决触发脉冲中固有的半带宽偏移。此外,在预测需要绝对速度测量的ODC时,具有较小单晶各向异性的合金对单晶弹性常数(SCEC)的依赖性更大。试图独立地确定这些弹性常数,以努力改善超声衍生的ODC与衍射衍生的ODC之间的相关性;容易获得使用超声非破坏性技术精确衍生铝合金中的ODC所需的更高的精度。超声衍生的ODC与中子和X射线的布拉格衍射技术的衍生显示出良好的相关性。当可以在ODC的推导中使用相对速度测量值时,显示出最佳的相关性。需要绝对速度测量的W400的派生结果并不是很好,但这是因为SCEC强烈地影响了这些推导。一旦针对所研究的特定合金独立确定了SCEC,W400的计算就得到了改进;具有六方晶体的材料中的ODC的计算也可以完成。由于微晶的对称性,可以使用超声技术提取更多信息,但是需要更多的物理测量。一些使用具有六方微晶材料的行业,例如锆合金和钛具有传统上使用的织构参数,这些参数提供了一些专门的织构度量。这些称为Kearns因子的纹理参数可以与ODC直接相关。再次,发现超声确定的ODC与衍射确定的ODC之间具有良好的相关性。此外,使用超声技术得出的Kearns参数与使用中子和X射线衍射得出的Kearns参数具有很好的相关性。

著录项

  • 作者

    Anderson, Alan Joseph;

  • 作者单位
  • 年度 1997
  • 总页数
  • 原文格式 PDF
  • 正文语种 en
  • 中图分类

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